Sodium phenolate and acetophenone can be obtained by adding sodium hydrate into azeotrope.
共沸物中加入氢化钠,分离出
钠盐和
乙酮。
Sodium phenolate and acetophenone can be obtained by adding sodium hydrate into azeotrope.
共沸物中加入氢化钠,分离出
钠盐和
乙酮。
Phenoxyacetophenone could be prepared from potassium phenolate and m bromoacetophenone via Ullmann reaction catalyzed by copper acetate in high yields.
基
乙酮可由
钾与
溴
乙酮在醋酸铜催化下以高产率合成。
The primary synthetic methods of 4-hydroxycoumarin was reviewed starting from phenol, 2-acetylsalicylic acid, methyl salicylate, and o-hydroxyacetophenone respectively.
概述了4-羟基香豆素合成方法,重点介绍了
法,乙酰水杨酸法,水杨酸甲酯法,邻羟基
乙酮法。
The phenols were O-alkylated with 100% conversion and 100% selectivities using phenacyl bromide and benzyl bromide as alkylating reagents.
用溴代乙酮和溴苄为烷基化试剂,以高产率和100%
转化率以及100%
性得到了
O-烷基化产物。
P-hydroxyacetophenone combined with methyl chloroacetate can get a new acetonate.This new acetonate combined with another compound-ethanolamine and get a new schiff base.
由对羟基乙酮与氯乙酸甲酯反应,得到一种酮,这种酮再与乙醇胺反应得到一种新
希夫碱。
Firstly, p-methylacetophenone was obtained in the presence of alchlor as the catalyst, and the optimum condition was 4:1:2 in molar ratio for toluene, acetic anhydride and alchlor with yield of 86.2%.
首先,以甲和乙酸酐为原料,在催化剂三氯化铝存在下合成对甲基
乙酮,并确定甲
,乙酸酐和三氯化铝
最佳摩尔比为4: 1: 2,收率为86.2%。
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