N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

苯胺和溴烷为原料,用四化铵作相转移催化剂,在常压下合成N,N二苯胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所得纤维素产品的含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

用四氯化胺作相转移催化剂可在常压下由苯胺和溴烷合成N,N-二苯胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

氯化二铝（DECA）和叠氮化钠为原料合成二叠氮铝（DEAA）时，反应介质的溶剂性质不同，产物及其收率也不同。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

碳二酯(DEC)为化试剂,与苯酚在气固相条件下催化合成苯醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

BTEAC(苄三氯化铵)为相转移催化剂合成了异烟酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三苯-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲）-苯酚等，这为进一步开发利用蒌蒿提供了科学依据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附和催化剂载体功能的多孔结构活性，纤维素为材料用相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)和化苦参碱(OMT)分别对二亚硝胺(DEN)诱发大鼠肝癌的预防阻断作用。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

二胺和二硫化碳为原料,经双水(275%)化,一步合成了四秋兰姆化二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

对氟苯酚和3-氯丙为起始原料,用苄三氯化铵作为催化剂,经过相转移催化合成对氟苯丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰化反应,使木粉转化成为热塑性材料,再与短切剑麻纤维混合,热压制得植物纤维增强塑化植物纤维复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷及双甲甲酯取代的两种双二硫代亚四硫代富瓦烯(BEDT-TTF)的衍生物及其它们与TCNQ的CT-络合物。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

用新的催化体系(铁-锑复合催化剂)催化三铝(TEA)与溴甲烷进行烷交换反应合成三甲铝(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗品通过精制工艺的改进,采用硫化钠和化钠的混合物进行处理,得到纯度≥99%的O,O-二硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采用纤维素与过量的氯烷及化钠反应,甲苯为稀释剂,用一步法成功地合成了纤维素。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

7-色醇和3-代戊甲酯为起始原料,甲醇为溶剂,合成了依托度.采用混合溶剂对粗品进行精制,得到了高纯度的依托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了麦芽酚、麦芽酚生产中的碱式溴化镁废渣为原料制取溴;溴、硫和醇合成溴烷的方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨磺）合成的新工艺：用氨醇硫酯与亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

用一种新型催化剂合成二甲苯原酯(DPCA),并简化了合成工艺,减少了生产过程中产生的三废,因而投入生产已具备了必要条件。这种新型催化剂可用于其它原酯类香料的合成。

N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

以苯胺和溴乙烷为原料,四乙基氢氧化铵作相转移催化剂,在常压下合成N,N二乙基苯胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所得乙基纤维素乙氧基含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

四乙基氯化胺作相转移催化剂可在常压下由苯胺和溴乙烷合成N,N-二乙基苯胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

以氯化二乙基铝（DECA）和叠氮化钠为原料合成二乙基叠氮铝（DEAA）时，反应介质溶剂性质不同，物及其收率也不同。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

以碳二乙酯(DEC)为乙基化试剂,与苯酚在气固相条件下催化合成苯乙醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

以BTEAC(苄基三乙基氯化铵)为相转移催化剂合成了异烟乙酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三苯基-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲乙基）-苯酚等，这为进一步开发利提供了科学依据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附和催化剂载体功能多孔结构活性炭，以乙基纤维素为材料相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)和氧化苦参碱(OMT)分别对二乙基亚硝胺(DEN)诱发大鼠肝癌预防阻断作。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

以二乙胺和二硫化碳为原料,经双氧水(275%)氧化,一步合成了四乙基秋兰姆化二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

以对氟苯酚和3-氯丙为起始原料,苄基三乙基氯化铵作为催化剂,经过相转移催化合成对氟苯氧丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰乙基化反应,使木粉转化成为热塑性材料,再与短切剑麻纤维混合,热压制得植物纤维增强塑化植物纤维基复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷基及双甲甲酯基取代两种双二硫代亚乙基四硫代富瓦烯(BEDT-TTF)衍生物及其它们与TCNQCT-络合物。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

新催化体系(铁-锑复合催化剂)催化三乙基铝(TEA)与溴甲烷进行烷基交换反应合成三甲基铝(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗通过精制工艺改进,采硫化钠和氢氧化钠混合物进行处理,得到纯度≥99%O,O-二乙基硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采纤维素与过量氯乙烷及氢氧化钠反应,以甲苯为稀释剂,一步法成功地合成了乙基纤维素。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

以7-乙基色醇和3-氧代戊甲酯为起始原料,以甲醇为溶剂,合成了依托度.采混合溶剂对粗进行精制,得到了高纯度依托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了以麦芽酚、乙基麦芽酚生中碱式溴化镁废渣为原料制取溴;以溴、硫和乙醇合成溴乙烷方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨乙基磺）合成新工艺：氨基乙醇硫酯与亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

一种新型催化剂合成乙二甲基苯乙基原酯(DPCA),并简化了合成工艺,减少了生过程中生三废,因而投入生已具备了必要条件。这种新型催化剂可于其它原酯类香料合成。

N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

以胺和溴乙烷为原料,用四乙基氢氧化铵作相转移催化剂,在常压下合成N,N二乙基胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所得乙基纤维素品的乙氧基含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

用四乙基氯化胺作相转移催化剂可在常压下由胺和溴乙烷合成N,N-二乙基胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

以氯化二乙基铝（DECA）和叠氮化钠为原料合成二乙基叠氮铝（DEAA）时，反应介质的溶剂性质不，及其收率也不。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

以碳二乙酯(DEC)为乙基化试剂,在气固相条件下催化合成乙醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

以BTEAC(苄基三乙基氯化铵)为相转移催化剂合成了异烟乙酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三基-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲乙基）-等，这为进一步开发利用蒌蒿提供了科学依据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附和催化剂载体功能的多孔结构活性炭，以乙基纤维素为材料用相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)和氧化苦参碱(OMT)分别对二乙基亚硝胺(DEN)诱发大鼠肝癌的预防阻断作用。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

以二乙胺和二硫化碳为原料,经双氧水(275%)氧化,一步合成了四乙基秋兰姆化二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

以对氟和3-氯丙为起始原料,用苄基三乙基氯化铵作为催化剂,经过相转移催化合成对氟氧丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰乙基化反应,使木粉转化成为热塑性材料,再短切剑麻纤维混合,热压制得植纤维增强塑化植纤维基复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷基及双甲甲酯基取代的两种双二硫代亚乙基四硫代富瓦烯(BEDT-TTF)的衍生及其它们TCNQ的CT-络合。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

用新的催化体系(铁-锑复合催化剂)催化三乙基铝(TEA)溴甲烷进行烷基交换反应合成三甲基铝(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗品通过精制工艺的改进,采用硫化钠和氢氧化钠的混合进行处理,得到纯度≥99%的O,O-二乙基硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采用纤维素过量的氯乙烷及氢氧化钠反应,以甲为稀释剂,用一步法成功地合成了乙基纤维素。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

以7-乙基色醇和3-氧代戊甲酯为起始原料,以甲醇为溶剂,合成了依托度.采用混合溶剂对粗品进行精制,得到了高纯度的依托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了以麦芽、乙基麦芽生中的碱式溴化镁废渣为原料制取溴;以溴、硫和乙醇合成溴乙烷的方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨乙基磺）合成的新工艺：用氨基乙醇硫酯亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

用一种新型催化剂合成乙二甲基乙基原酯(DPCA),并简化了合成工艺,减少了生过程中生的三废,因而投入生已具备了必要条件。这种新型催化剂可用于其它原酯类香料的合成。

N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

以苯胺和溴乙烷为原料,用四乙基氢氧化铵作相转移催化剂,在常压下合成N,N二乙基苯胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所得乙基纤品的乙氧基含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

用四乙基氯化胺作相转移催化剂可在常压下由苯胺和溴乙烷合成N,N-二乙基苯胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

以氯化二乙基铝（DECA）和叠氮化钠为原料合成二乙基叠氮铝（DEAA）时，反应介质的溶剂性质不同，物及其收率也不同。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

以碳二乙酯(DEC)为乙基化试剂,与苯酚在气固相条件下催化合成苯乙醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

以BTEAC(苄基三乙基氯化铵)为相转移催化剂合成了异烟乙酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三苯基-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲乙基）-苯酚等，这为进一步开发利用蒌了科学依据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附和催化剂载体功能的多孔结构活性炭，以乙基纤为材料用相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)和氧化苦参碱(OMT)分别对二乙基亚硝胺(DEN)诱发大鼠肝癌的预防阻断作用。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

以二乙胺和二硫化碳为原料,经双氧水(275%)氧化,一步合成了四乙基秋兰姆化二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

以对氟苯酚和3-氯丙为起始原料,用苄基三乙基氯化铵作为催化剂,经过相转移催化合成对氟苯氧丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰乙基化反应,使木粉转化成为热塑性材料,再与短切剑麻纤混合,热压制得植物纤增强塑化植物纤基复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷基及双甲甲酯基取代的两种双二硫代亚乙基四硫代富瓦烯(BEDT-TTF)的衍生物及其它们与TCNQ的CT-络合物。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

用新的催化体系(铁-锑复合催化剂)催化三乙基铝(TEA)与溴甲烷进行烷基交换反应合成三甲基铝(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗品通过精制工艺的改进,采用硫化钠和氢氧化钠的混合物进行处理,得到纯度≥99%的O,O-二乙基硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采用纤与过量的氯乙烷及氢氧化钠反应,以甲苯为稀释剂,用一步法成功地合成了乙基纤。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

以7-乙基色醇和3-氧代戊甲酯为起始原料,以甲醇为溶剂,合成了依托度.采用混合溶剂对粗品进行精制,得到了高纯度的依托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了以麦芽酚、乙基麦芽酚生中的碱式溴化镁废渣为原料制取溴;以溴、硫和乙醇合成溴乙烷的方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨乙基磺）合成的新工艺：用氨基乙醇硫酯与亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

用一种新型催化剂合成乙二甲基苯乙基原酯(DPCA),并简化了合成工艺,减少了生过程中生的三废,因而投入生已具备了必要条件。这种新型催化剂可用于其它原酯类香料的合成。

N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

以胺和溴乙烷为原料,用四乙基氢氧化铵作相转移催化剂,在常压下合成N,N二乙基胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所得乙基纤维素品的乙氧基含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

用四乙基氯化胺作相转移催化剂可在常压下由胺和溴乙烷合成N,N-二乙基胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

以氯化二乙基铝（DECA）和叠氮化钠为原料合成二乙基叠氮铝（DEAA）时，反应介质的溶剂性质不，及其收率也不。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

以碳二乙酯(DEC)为乙基化试剂,在气固相条件下催化合成乙醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

以BTEAC(苄基三乙基氯化铵)为相转移催化剂合成了异烟乙酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三基-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲乙基）-等，这为进一步开发利用蒌蒿提供了科学依据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附和催化剂载体功能的多孔结构活性炭，以乙基纤维素为材料用相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)和氧化苦参碱(OMT)分别对二乙基亚硝胺(DEN)诱发大鼠肝癌的预防阻断作用。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

以二乙胺和二硫化碳为原料,经双氧水(275%)氧化,一步合成了四乙基秋兰姆化二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

以对氟和3-氯丙为起始原料,用苄基三乙基氯化铵作为催化剂,经过相转移催化合成对氟氧丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰乙基化反应,使木粉转化成为热塑性材料,再短切剑麻纤维混合,热压制得植纤维增强塑化植纤维基复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷基及双甲甲酯基取代的两种双二硫代亚乙基四硫代富瓦烯(BEDT-TTF)的衍生及其它们TCNQ的CT-络合。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

用新的催化体系(铁-锑复合催化剂)催化三乙基铝(TEA)溴甲烷进行烷基交换反应合成三甲基铝(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗品通过精制工艺的改进,采用硫化钠和氢氧化钠的混合进行处理,得到纯度≥99%的O,O-二乙基硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采用纤维素过量的氯乙烷及氢氧化钠反应,以甲为稀释剂,用一步法成功地合成了乙基纤维素。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

以7-乙基色醇和3-氧代戊甲酯为起始原料,以甲醇为溶剂,合成了依托度.采用混合溶剂对粗品进行精制,得到了高纯度的依托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了以麦芽、乙基麦芽生中的碱式溴化镁废渣为原料制取溴;以溴、硫和乙醇合成溴乙烷的方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨乙基磺）合成的新工艺：用氨基乙醇硫酯亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

用一种新型催化剂合成乙二甲基乙基原酯(DPCA),并简化了合成工艺,减少了生过程中生的三废,因而投入生已具备了必要条件。这种新型催化剂可用于其它原酯类香料的合成。

N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

苯胺和溴乙烷为原料,用四乙基铵作相转移催剂,在常压下合成N,N二乙基苯胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所得乙基纤维素产品的乙基含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

用四乙基氯胺作相转移催剂可在常压下由苯胺和溴乙烷合成N,N-二乙基苯胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

氯二乙基铝（DECA）和叠氮钠为原料合成二乙基叠氮铝（DEAA）时，反应介质的溶剂质不同，产物及其收率也不同。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

碳二乙酯(DEC)为乙基试剂,与苯酚在气固相条件下催合成苯乙醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

BTEAC(苄基三乙基氯铵)为相转移催剂合成了异烟乙酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三苯基-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲乙基）-苯酚等，这为进一步开发利用蒌蒿提供了科学依据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附和催剂载体功能的多孔结构活，乙基纤维素为材料用相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)和苦参碱(OMT)分别对二乙基亚硝胺(DEN)诱发大鼠肝癌的预防阻断作用。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

二乙胺和二硫碳为原料,经双水(275%),一步合成了四乙基秋兰姆二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

对氟苯酚和3-氯丙为起始原料,用苄基三乙基氯铵作为催剂,经过相转移催合成对氟苯丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰乙基反应,使木粉转成为热塑材料,再与短切剑麻纤维混合,热压制得植物纤维增强塑植物纤维基复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷基及双甲甲酯基取代的两种双二硫代亚乙基四硫代富瓦烯(BEDT-TTF)的衍生物及其它们与TCNQ的CT-络合物。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

用新的催体系(铁-锑复合催剂)催三乙基铝(TEA)与溴甲烷进行烷基交换反应合成三甲基铝(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗品通过精制工艺的改进,采用硫钠和钠的混合物进行处理,得到纯度≥99%的O,O-二乙基硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采用纤维素与过量的氯乙烷及钠反应,甲苯为稀释剂,用一步法成功地合成了乙基纤维素。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

7-乙基色醇和3-代戊甲酯为起始原料,甲醇为溶剂,合成了依托度.采用混合溶剂对粗品进行精制,得到了高纯度的依托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了麦芽酚、乙基麦芽酚生产中的碱式溴镁废渣为原料制取溴;溴、硫和乙醇合成溴乙烷的方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨乙基磺）合成的新工艺：用氨基乙醇硫酯与亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

用一种新型催剂合成乙二甲基苯乙基原酯(DPCA),并简了合成工艺,减少了生产过程中产生的三废,因而投入生产已具备了必要条件。这种新型催剂可用于其它原酯类香料的合成。

N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

以苯胺和溴烷为原料,四基氢氧化铵作相转移催化剂,在常压下合成N,N二基苯胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所得基纤维素产氧基含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

四基氯化胺作相转移催化剂可在常压下由苯胺和溴烷合成N,N-二基苯胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

以氯化二基铝（DECA）和叠氮化钠为原料合成二基叠氮铝（DEAA）时，反应介质溶剂性质不同，产物及其收率也不同。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

以碳二酯(DEC)为基化试剂,与苯酚在气固相条件下催化合成苯醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

以BTEAC(苄基三基氯化铵)为相转移催化剂合成了异烟酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三苯基-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲基）-苯酚等，这为进一步开发蒿提供了科学依据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附和催化剂载体功能多孔结构活性炭，以基纤维素为材料相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)和氧化苦参碱(OMT)分别对二基亚硝胺(DEN)诱发大鼠肝癌预防阻断作。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

以二胺和二硫化碳为原料,经双氧水(275%)氧化,一步合成了四基秋兰姆化二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

以对氟苯酚和3-氯丙为起始原料,苄基三基氯化铵作为催化剂,经过相转移催化合成对氟苯氧丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰基化反应,使木粉转化成为热塑性材料,再与短切剑麻纤维混合,热压制得植物纤维增强塑化植物纤维基复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷基及双甲甲酯基取代两种双二硫代亚基四硫代富瓦烯(BEDT-TTF)衍生物及其它们与TCNQCT-络合物。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

新催化体系(铁-锑复合催化剂)催化三基铝(TEA)与溴甲烷进行烷基交换反应合成三甲基铝(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗通过精制工艺改进,采硫化钠和氢氧化钠混合物进行处理,得到纯度≥99%O,O-二基硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采纤维素与过量氯烷及氢氧化钠反应,以甲苯为稀释剂,一步法成功地合成了基纤维素。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

以7-基色醇和3-氧代戊甲酯为起始原料,以甲醇为溶剂,合成了依托度.采混合溶剂对粗进行精制,得到了高纯度依托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了以麦芽酚、基麦芽酚生产中碱式溴化镁废渣为原料制取溴;以溴、硫和醇合成溴烷方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨基磺）合成新工艺：氨基醇硫酯与亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

一种新型催化剂合成二甲基苯基原酯(DPCA),并简化了合成工艺,减少了生产过程中产生三废,因而投入生产已具备了必要条件。这种新型催化剂可于其它原酯类香料合成。

N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

以苯胺溴乙烷为原料,用四乙氢氧铵作相转剂,在常压下合成N,N二乙苯胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所得乙纤维素产品的乙氧含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

用四乙氯胺作相转剂可在常压下由苯胺溴乙烷合成N,N-二乙苯胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

以氯二乙（DECA）叠氮钠为原料合成二乙叠氮（DEAA）时，反应介质的溶剂性质不同，产物及其收率也不同。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

以碳二乙酯(DEC)为乙试剂,与苯酚在气固相条件下合成苯乙醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

以BTEAC(苄三乙氯铵)为相转剂合成了异烟乙酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三苯-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲乙）-苯酚等，这为进一步开发利用蒌蒿提供了科学依据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附剂载体功能的多孔结构活性炭，以乙纤维素为材料用相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)氧苦参碱(OMT)分别对二乙亚硝胺(DEN)诱发大鼠肝癌的预防阻断作用。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

以二乙胺二硫碳为原料,经双氧水(275%)氧,一步合成了四乙秋兰姆二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

以对氟苯酚3-氯丙为起始原料,用苄三乙氯铵作为剂,经过相转合成对氟苯氧丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰乙反应,使木粉转成为热塑性材料,再与短切剑麻纤维混合,热压制得植物纤维增强塑植物纤维复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷及双甲甲酯取代的两种双二硫代亚乙四硫代富瓦烯(BEDT-TTF)的衍生物及其它们与TCNQ的CT-络合物。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

用新的体系(铁-锑复合剂)三乙(TEA)与溴甲烷进行烷交换反应合成三甲(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗品通过精制工艺的改进,采用硫钠氢氧钠的混合物进行处理,得到纯度≥99%的O,O-二乙硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采用纤维素与过量的氯乙烷及氢氧钠反应,以甲苯为稀释剂,用一步法成功地合成了乙纤维素。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

以7-乙色醇3-氧代戊甲酯为起始原料,以甲醇为溶剂,合成了依托度.采用混合溶剂对粗品进行精制,得到了高纯度的依托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了以麦芽酚、乙麦芽酚生产中的碱式溴镁废渣为原料制取溴;以溴、硫乙醇合成溴乙烷的方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨乙磺）合成的新工艺：用氨乙醇硫酯与亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

用一种新型剂合成乙二甲苯乙原酯(DPCA),并简了合成工艺,减少了生产过程中产生的三废,因而投入生产已具备了必要条件。这种新型剂可用于其它原酯类香料的合成。

N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.

以苯胺和溴烷为原料,用四氢氧化铵作相转移催化剂,在常压下合成N,N二苯胺。

The content of ethoxyl group in obtained product was 43.98%.

该法所纤维素产品的氧含量为43.98%。

N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.

用四氯化胺作相转移催化剂可在常压下由苯胺和溴烷合成N,N-二苯胺。

The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.

以氯化二铝（DECA）和叠氮化钠为原料合成二叠氮铝（DEAA）时，反应介质的溶剂性质不同，产物及其收率也不同。

Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.

以碳二酯(DEC)为化试剂,与苯酚在气固相条件下催化合成苯醚。

Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.

以BTEAC(苄三氯化铵)为相转移催化剂合成了异烟酯。

The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.

其主要成分是三苯-甲烷、叶绿醇、正十六碳、2,4,6-三（1,1-二甲）-苯酚等，这为进一步开发利用蒌蒿提供了据。

Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.

摘要对兼具吸附和催化剂载体功能的多孔结构活性炭，以纤维素为材料用相分离进行包覆。

Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).

研究苦参碱(MT)和氧化苦参碱(OMT)分别对二亚硝胺(DEN)诱发大鼠肝癌的预防阻断作用。

Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.

以二胺和二硫化碳为原料,经双氧水(275%)氧化,一步合成了四秋兰姆化二硫。

The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.

以对氟苯酚和3-氯丙为起始原料,用苄三氯化铵作为催化剂,经过相转移催化合成对氟苯氧丙。

By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.

通过氰化反应,使木粉转化成为热塑性材料,再与短切剑麻纤维混合,热压制植物纤维增强塑化植物纤维复合材料。

Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.

合成了带双羟烷及双甲甲酯取代的两种双二硫代亚四硫代富瓦烯(BEDT-TTF)的衍生物及其它们与TCNQ的CT-络合物。

Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.

用新的催化体系(铁-锑复合催化剂)催化三铝(TEA)与溴甲烷进行烷交换反应合成三甲铝(TMA)。

The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗品通过精制工艺的改进,采用硫化钠和氢氧化钠的混合物进行处理,到纯度≥99%的O,O-二硫代磷酰氯。

Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.

采用纤维素与过量的氯烷及氢氧化钠反应,以甲苯为稀释剂,用一步法成功地合成了纤维素。

Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.

以7-色醇和3-氧代戊甲酯为起始原料,以甲醇为溶剂,合成了托度.采用混合溶剂对粗品进行精制,到了高纯度的托度.

The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.

研究了以麦芽酚、麦芽酚生产中的碱式溴化镁废渣为原料制取溴;以溴、硫和醇合成溴烷的方法。

This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.

研究了牛磺（2-氨磺）合成的新工艺：用氨醇硫酯与亚硫钠溶液反应制备，收率达85％。

Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.

用一种新型催化剂合成二甲苯原酯(DPCA),并简化了合成工艺,减少了生产过程中产生的三废,因而投入生产已具备了必要条件。这种新型催化剂可用于其它原酯类香料的合成。